期刊
JOURNAL OF BIOCHEMICAL AND BIOPHYSICAL METHODS
卷 70, 期 2, 页码 117-131出版社
ELSEVIER SCIENCE BV
DOI: 10.1016/j.jbbm.2006.10.010
关键词
solid-phase extraction; solid-phase micro-extraction; hollow-fiber micro-extraction; stir-bar sorptive extraction; matrix solid-phase dispersion; food
Solid-phase extraction (SPE) procedures for pesticide residues in food and environment are reviewed and discussed. The use of these procedures, which include several approaches such as: matrix solid-phase dispersion (MSPD), solid-phase micro-extraction (SPME) and stir-bar sorptive extraction (SBSE), represents an opportunity to reduce analysis time, solvent consumption, and overall cost. SPE techniques differ from solvent extraction depending on the interactions between a sorbent and the pesticide. This interaction may be specific for a particular pesticide, as in the interaction with an immunosorbent, or non-specific, as in the way a number of different pesticides are adsorbed on apolar or polar materials. A variety of applications were classified according to the method applied: conventional SPE, SPME, hollow-fiber micro-extraction (HFME), MSPD and SBSE. Emphasis is placed on the multiresidue analysis of liquid and solid samples. (c) 2006 Elsevier B.V. All rights reserved.
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