期刊
ORGANIC PROCESS RESEARCH & DEVELOPMENT
卷 11, 期 3, 页码 598-604出版社
AMER CHEMICAL SOC
DOI: 10.1021/op600278f
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资金
- NIGMS NIH HHS [R01 GM072586, R01 GM072586-01A1] Funding Source: Medline
A series of cyclohexadienones were synthesized by dearomatization of phenols followed by Dess-Martin oxidation. Asymmetric intramolecular Stetter reactions of these substrates provide hydrobenzofuranones in good to excellent yields and excellent stereoselectivities. Up to three stereocenters as well as a quaternary stereocenter are formed from polysubstituted substrates. A scale-up experiment demonstrates the utility of this transformation.
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