期刊
JOURNAL OF ORGANIC CHEMISTRY
卷 72, 期 10, 页码 3969-3971出版社
AMER CHEMICAL SOC
DOI: 10.1021/jo070246n
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[GRAPHICS] A facile and general protocol for the preparation of isothiocyanates from alkyl and aryl amines is reported. This method relies on a tosyl chloride mediated decomposition of a dithiocarbamate salt that is generated in situ by treatment of an amine with carbon disulfide and triethylamine. Utilizing this protocol, we have prepared 19-alkyl- and arylisothiocyanates in moderate to excellent yield.
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