期刊
TETRAHEDRON LETTERS
卷 48, 期 21, 页码 3731-3734出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2007.03.089
关键词
macroporous polystyrene-supported IBX amide; MPS-IBX resin; polymer-supported reagent; oxidation
In this study, macroporous polystyrene-supported IBX (MPS-IBX) amides were prepared in two simple steps, and the polymeric reagent was then evaluated for its efficiency in converting a range of alcohols to the corresponding carbonyl compounds in various solvents. The results indicated that the MPS-IBX amides were compatible with a variety of solvents, and had a more efficient oxidation activity toward alkyl alcohols than the gel type polystyrene-supported IBX amides. Finally, the resin that was consumed in the oxidation reaction was regenerated to give a restored loading level of 0.44-0.54 mmol/g. (c) 2007 Elsevier Ltd. All rights reserved.
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