期刊
ANALYTICAL SCIENCES
卷 26, 期 4, 页码 455-459出版社
JAPAN SOC ANALYTICAL CHEMISTRY
DOI: 10.2116/analsci.26.455
关键词
-
资金
- Ministry of Science and Technology of China [2009ZX09502-27]
- Science and Technology Development Foundation of Tianjin Colleges and Universities [2006ZD19]
Hydrophobic task specific ionic liquid (TSIL) functionalized 2-mercaptobenzothiazole (MBT) was synthesized and characterized by NMR and HRMS. The capability of TSIL-MBT for the selective separation and preconcentration of Cd2+, which was determined by flame atomic absorption spectrometry (FAAS) from water and food samples, was investigated. The TSIL-MBT with high selectivity for the extraction of Cd2+ was discussed by comparing with a traditional extractant, such as ammonium pyrrolidine dithiocarbamate (APDC) and diethydithiocarbamate (DDTC), and the recoveries of the extraction Cd2+ by TSIL-MBT were much better than APDC and DDTC. The proposed method was evaluated by analyzing two certified reference materials. The Cd2+ concentration, determined by the developed methodology, was in good agreement with certified values.
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