期刊
ANALYTICAL SCIENCES
卷 24, 期 2, 页码 267-271出版社
JAPAN SOC ANALYTICAL CHEMISTRY
DOI: 10.2116/analsci.24.267
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A 5-amino-8-hydroxyquinoline (AHQ)-modified gold nanoparticle (GNP) layer was fabricated on an inner wall of a silica capillary column by alternatively passing a citrate-stabilized GNP solution and an AHQ solution in a repeating fashion. The observations by a field emission scanning electron microscope showed that the thickness of the resulting GNP layer was about 0.15 mu m. This column was then used as an open tubular solid-phase extraction column for cadmium, followed by electrothermal atomic absorption spectrometric determination. The detection limit of 0.009 ng ml(-1) was obtained.
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