期刊
JOURNAL OF COATINGS TECHNOLOGY AND RESEARCH
卷 4, 期 2, 页码 131-138出版社
SPRINGER
DOI: 10.1007/s11998-007-9015-2
关键词
atomic force microscopy; polyurethanes; silicones; thermoset
High throughput combinatorial characterization was performed on thermosetting siloxane-urethane coatings in order to find a correlation between the characterization techniques, surface topography, and adhesion strength of barnacles. A series of coatings having microtopographical surfaces with different domain sizes were prepared based on a thermosetting siloxane-urethane system. This microtopography was formed spontaneously during the film-formation process. These surfaces were characterized by atomic force microscopy (AFM), surface energy, dynamic contact angle, and pseudo barnacle pull-off a adhesion and were compared to pure polyurethane (PU) and silicone rubber control. Surface energy and dynamic contact angles were measured by an automated surface energy measurement system and pull-off adhesion values were obtained from a high throughput pull-off adhesion measurement unit. The results were compared with the adhesion strength of barnacles.
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