期刊
ANALYTICAL METHODS
卷 4, 期 4, 页码 1160-1162出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c2ay05898g
关键词
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资金
- Steel Foundation for the Environmental Protection Technology (SEPT) [C-33-26, C-30-25]
- Grants-in-Aid for Scientific Research [23350030] Funding Source: KAKEN
A novel pre-separation technique for the determination of divalent trace heavy metals in a soil sample was developed, in which deferoxamine was used as a masking agent for trivalent metal ions, Al3+ and Fe3+, and a chelate column was applied to collect target heavy metal ions and to eliminate alkali metal and alkaline earth metal ions. Deferoxamine had such a strong and selective masking effect on Al3+ and Fe3+ that divalent trace heavy metals in the soil sample were well separated from considerably greater amounts of Al3+ and Fe3+. Consequently, the determination of four trace metals (Ni, Cu, Zn, and Pb) in a certified soil reference material (JSAC-0401) was successfully performed using electrospray ionization mass spectrometry (ESIMS).
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