期刊
ANALYTICAL LETTERS
卷 43, 期 16, 页码 2563-2571出版社
TAYLOR & FRANCIS INC
DOI: 10.1080/00032711003731381
关键词
Dispersive liquid-liquid microextraction; Electrothermal atomic absorption spectrometry; Preconcentration; Speciation of antimony
资金
- Research Council of University of Tehran
Dispersive liquid-liquid microextraction (DLLME) technique combined with electrothermal atomic absorption spectrometry (ET-AAS) was proposed for determination of antimony(III) and total antimony at very low concentrations in water samples. The N-benzoyl-N-phenylhydroxylamine (BPHA) was used as a chelating agent, and chloroform and ethanol were used as extraction and disperser solvents, respectively. The effect of various experimental parameters on the extraction and determination was investigated. The detection limits (3 sigma) were 0.005gL-1 for Sb(III) and 0.008gL-1 for total Sb. The developed method was applied successfully to the determination of Sb(III) and total Sb in natural water samples.
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