期刊
SYNTHESIS-STUTTGART
卷 -, 期 16, 页码 2529-2533出版社
GEORG THIEME VERLAG KG
DOI: 10.1055/s-2007-983817
关键词
oxidation; oxygen; methyl heteroaryls; benzyl anion; benzyl alcohols
Oxidation of nitrogen-based methyl heteroaryls with molecular oxygen resulted in the formation of the corresponding benzyl alcohols. While experimentally easy and amenable to large-scale preparations, this approach has limitations with respect to the particular nature of heterocyclic substrates. Using this methodology, the title compound, 2-[N-(tert-butoxycarbonyl)amino]-4-pyridinecarbaldehyde, considered to be a versatile pharmaceutical intermediate, was prepared on a multigram scale.
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