期刊
JOURNAL OF ORGANIC CHEMISTRY
卷 72, 期 18, 页码 7050-7053出版社
AMER CHEMICAL SOC
DOI: 10.1021/jo071126i
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资金
- NIGMS NIH HHS [GM R01-30938] Funding Source: Medline
A novel gamma-selective conjugate addition of 1-silyl-substituted dienol ethers to nitroalkenes activated by Lewis acids has been developed. The resulting alpha,beta-unsaturated acylsilanes undergo photoinduced protodesilylation to afford the corresponding enals, which can be conveniently transformed into azepanes under appropriate reductive conditions.
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