期刊
STEROIDS
卷 72, 期 11-12, 页码 736-739出版社
ELSEVIER SCIENCE INC
DOI: 10.1016/j.steroids.2007.06.002
关键词
synthesis; fused steroids; pyridines; X-ray
The preparation of pyridine rings fused to the 3,4-positions of the steroid nucleus is herein described. These new pyridine derivatives were prepared in good yields by the reaction of propargylamine with 17 beta-hydroxyandrost-4- en-3 -one, 17 alpha-methyl-17p-hydroxyandrost-4en-3-one, 17 beta-hydroxyestr-4-en-3-one catalyzed by Cu(II). The structure of 17 beta-hydroxy-5ene-androst-3-ene[3,4-b]pyridine was determined by X-ray analysis.
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