期刊
TETRAHEDRON LETTERS
卷 48, 期 42, 页码 7469-7471出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2007.08.074
关键词
thiols; disulfides; oxidation; cerium chloride; iodine; graphite
A very simple procedure for the efficient oxidation of thiols to disulfides catalyzed by I-2/CeCl3 center dot 7H(2)O in graphite and ethyl acetate as the solvent, in an open system at room temperature is described. The reaction proceeds cleanly under mild conditions and was performed with aromatic, aliphatic, and heterocyclic thiols. (C) 2007 Elsevier Ltd. All rights reserved.
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