期刊
APPLIED SPECTROSCOPY
卷 61, 期 11, 页码 1178-1183出版社
SOC APPLIED SPECTROSCOPY
DOI: 10.1366/000370207782597148
关键词
near-infrared spectroscopy; NIRS; dispersive spectroscopy; Fourier transform near-infrared spectroscopy; FT-NIR spectroscopy; barley; fuel ethanol; partial least squares; PLS regression
The objective of this study was to explore the potential of near-infrared spectroscopy for determining the compositional quality properties of barley as a feedstock for fuel ethanol production and to compare the prediction accuracy between calibration models obtained using a Fourier transform near-infrared system (FT-NIR) and a dispersive near-infrared system. The total sample set contained 206 samples of three types of barley, hull-less, malt, and hulled varieties, which were grown at various locations in the eastern U.S. from 2002 to 2005 years. A new hull-less barley variety, Doyce, which was specially bred for potential use in ethanol production, was included in the sample set. One hundred and thirty-eight barley samples were used for calibration and sixty-eight were used for validation. Ground barley samples were scanned on both a FTNIR spectrometer (10000 to 4000 cm(-1) at 4 cm(-1) resolution) and a dispersive NIR spectrometer (400 to 2498 nm at 10 nm resolution), respectively. Six grain components, moisture, starch, P-glucan, protein, oil, and ash content, were analyzed as parameters of barley quality. Principal component analysis showed that barley samples could be classified by their types: hull-less, malt, and hulled. Partial least squares regression indicated that both FT-NIR and dispersive NIR spectroscopy have the potential to determine quality properties of barley with an acceptable accuracy, except for for beta- glucan content. There was no predictive advantage in using a high-resolution FT-NIR instrument over a dispersive system for most components of barley.
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