期刊
JOURNAL OF ORGANIC CHEMISTRY
卷 72, 期 23, 页码 8987-8989出版社
AMER CHEMICAL SOC
DOI: 10.1021/jo701665j
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资金
- NCI NIH HHS [N02 CB56603] Funding Source: Medline
[GRAPHICS] A highly efficient and general method for Suzuki cross-coupling reaction en route to the synthesis of polycyclic aromatic hydrocarbons (PAHs) and their metabolites has been developed. Microwave irradiation of aryl bromides 1 and boronic acids (2 and 3) using polyurea microencapsulated palladium catalyst (Pd EnCat 30) gave the coupling adducts 4 and 5 in excellent yields in just 20 min compared to similar to 24 h under thermal conditions, corresponding to a similar to 72-fold increase in reaction rate.
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