期刊
BULLETIN OF THE CHEMICAL SOCIETY OF JAPAN
卷 80, 期 11, 页码 2213-2219出版社
CHEMICAL SOC JAPAN
DOI: 10.1246/bcsj.80.2213
关键词
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The reaction of arenes with elemental iodine, acetic acid, and potassium mu-peroxo-hexaoxodisulfate (K2S2O8) in the presence of concentrated sulfuric acid, efficiently generated the corresponding (diacetoxyiodo)arenes in good yields. Diaryliodonium triflates were directly synthesized by reaction of arenes with elemental iodine in good yields by using, K2S2O8, AcOH, and TfOH. Diaryliodonium tosylates were also prepared from arenes and elemental iodine by using K2S2O8, AcOH, H2SO4, and TsOH. The procedure involved mild conditions and a straightforward one-pot synthesis.
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