期刊
JOURNAL OF ORGANIC CHEMISTRY
卷 72, 期 24, 页码 9387-9390出版社
AMER CHEMICAL SOC
DOI: 10.1021/jo701509r
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[Graphics] An ester enolate rearrangement/silicon mediated fragmentation cascade was used to convert 7 and 8 into the alcohol 9. The alcohol 9 was converted into the allylic alcohol 12 and then to the ester 14. A further ester enolate rearrangement furnished the stereochemical identity of galbonolide B 1. Base mediated macrocyclization of the acetate ester 16 followed by base mediated alkylation and acetal deprotection gave galbonolide B 1.
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