期刊
APPLIED SURFACE SCIENCE
卷 254, 期 3, 页码 781-784出版社
ELSEVIER SCIENCE BV
DOI: 10.1016/j.apsusc.2007.05.086
关键词
combinatorial; thin films; reflectometry
The goal of the design of pulsed laser deposition (PLD) combinatorial library films is to optimize the compositional coverage of the films while maintaining a uniform thickness. The deposition pattern of excimer laser PLD films can be modeled with a bimodal cos(n) distribution. Deposited films were characterized using a spectroscopic reflectometer (250-1000 nm) to map the thickness of both single composition calibration films and combinatorial library films. These distribution functions were used to simulate the composition and thickness of multiple target combinatorial library films. The simulations were correlated with electron-probe microanalysis wavelength-dispersive spectroscopy (EPMA-WDS) composition maps. The composition and thickness of the library films can be fine-tuned by adjusting the laser spot size, fluence, background gas pressure, target geometry and other processing parameters which affect the deposition pattern. Results from compositionally graded combinatorial library films of the ternary system Al(2)O(3)-HfO(2)-Y(2)O(3) are discussed. (C) 2007 Elsevier B.V. All rights reserved.
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