期刊
REACTION KINETICS AND CATALYSIS LETTERS
卷 92, 期 2, 页码 293-302出版社
SPRINGER
DOI: 10.1007/s11144-007-5203-4
关键词
CL-20 synthesis; debenzylation; palladium-based catalyst; Pd/C deactivation
Polycyclic nitramine hexanitrohexaazaisowurtzitane (HNIW, CL-20) is synthesized via hydrodebenzylation of a precursor over palladium-based catalyst. In the present work, we studied the influence of the synthesis method of the palladium-based catalyst on the catalyst behavior during the hydrodebenzylation reaction of 2,4,6,8,10,12-hexabenzyl-2,4,6,8,10,12-hexaazatetracyclo[5.5.0.0(3,11).0(5,9)] dodecane.
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