期刊
JOURNAL OF THE CERAMIC SOCIETY OF JAPAN
卷 117, 期 1370, 页码 1115-1119出版社
CERAMIC SOC JAPAN-NIPPON SERAMIKKUSU KYOKAI
DOI: 10.2109/jcersj2.117.1115
关键词
Layered hydroxide zinc aminobenzoate compound; Layered basic metal salt; Exfoliation reaction; Nanosheet
资金
- Japan Society for the Promotion of Science [20350096]
- Shaanxi Provincial Natural Science Foundation of China [20071324]
- Grants-in-Aid for Scientific Research [20350096] Funding Source: KAKEN
Two types of layered hydroxide zinc o-aminobenzoate compounds with structures of layered basic metal salt (LBMS) were prepared by reacting of zinc hydroxide and o-aminobenzoic acid solution in a temperature range of 40-110 degrees C. The formation reactions, structures, chemical compositions, and exfoliation behavior in alcohol solvents of the layered compounds were investigated by using XRD, TG-DTA, SEM, and TEM. The layered phase with a basal spacing of 1.33 nm has an alpha-Ni(OH)(2)-like structure, and its chemical formula can be written as Zn(OH)(1.27)(o-NH2C6H4COO)(0.73)center dot H2O. The 1.33 nm layered phase shows plate-like particle morphology. The plate-like crystals can be exfoliated into nanosheet-like particles in alcohol solvents. (C)2009 The Ceramic Society of Japan. All rights reserved.
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