期刊
ADVANCED SYNTHESIS & CATALYSIS
卷 360, 期 17, 页码 3271-3276出版社
WILEY-V C H VERLAG GMBH
DOI: 10.1002/adsc.201800388
关键词
Phthalimides; Cobalt catalyst; C-H carbonylation; Benzoyl hydrazides; Hydrogenolysis
资金
- NSFC [21732001, 21672017, 21472072, 21290183]
- Shenzhen Science and Technology Innovation Committee [JCYJ20150529153646078, JSGG20160229150510483]
- Program for Changjiang Scholars and Innovative Research Team in University [PCSIRT: IRT_15R28]
- 111 Program of MOE
A cobalt-catalyzed C-H carbonylation of benzoyl hydrazides has been developed by using 2-(1-methylhydrazinyl)pyridine as the bidentate directing group. This transformation is mild, efficient, operationally simple, and highly functional-group-tolerant. The protocol has generated a broad range of phthalimide derivatives in good to excellent yields. The ligand moiety can be readily removed through hydrogenolysis.
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