期刊
ADVANCED SYNTHESIS & CATALYSIS
卷 360, 期 9, 页码 1800-1804出版社
WILEY-V C H VERLAG GMBH
DOI: 10.1002/adsc.201800161
关键词
Amidation; ball mill; cobalt; C-H bond functionalization; mechanosynthesis
资金
- China Scholarship Council (CSC)
- RWTH Aachen University from the Distinguished Professorship Program - Excellence Initiative of the German Federal Government
- RWTH Aachen University from the Distinguished Professorship Program - Excellence Initiative of the German State Government
Ball milling techniques have been applied in the development of a mechanosynthesis of [Cp*Co(CO)I-2], which proved highly efficient as catalyst in mechanochemical C-H bond amidations of indoles in a mixer ball mill. A wide range of amidated products is obtained in excellent yields. Compared to the solution-based methods, the procedure opens a more feasible and environmentally-friendly access to both the cobalt(III) catalyst and 2-amidated indoles.
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