期刊
ADVANCED SYNTHESIS & CATALYSIS
卷 357, 期 1, 页码 77-82出版社
WILEY-V C H VERLAG GMBH
DOI: 10.1002/adsc.201400767
关键词
boron; catalysis; dehydrogenation; Lewis acids; multiple bonds
Under zinc Lewis acid catalysis, terminal alkynes coupled dehydrogenatively with 1,8-naphthalenediaminatoborane [HB(dan)]. It is important to note that the resulting alkynylboranes with an C(sp)-B(dan) bond are isolable by column chromatography on silica gel (SiO2) and are usable as coupling partners for palladium- and copper-catalyzed cross-coupling reactions with (hetero) aryl halides.
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