期刊
ADVANCED SYNTHESIS & CATALYSIS
卷 354, 期 13, 页码 2438-2442出版社
WILEY-V C H VERLAG GMBH
DOI: 10.1002/adsc.201200345
关键词
aldehydes; C?H activation; copper; formylation; tertiary amines
资金
- National Natural Science Foundation of China [20972115]
- Natural Science Foundation of Zhejiang Province [R4110294]
- Priority Academic Program Development of Jiangsu Higher Education Institutions
A copper-catalyzed formylation reaction has been developed by employing oxygen (O2) as the clean oxidant. The C?H bonds of indoles were C-3-formylated by tetramethylethylenediamine (TMEDA) and water (H2O; in situ formed and external added water) as the carbonyl source in moderate to good yields with good functional group tolerance. Thus, it represents a facile procedure leading to 3-formylindoles.
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