期刊
ADVANCED SYNTHESIS & CATALYSIS
卷 353, 期 4, 页码 580-584出版社
WILEY-V C H VERLAG GMBH
DOI: 10.1002/adsc.201000791
关键词
azides; click chemistry; desulfanylation; difluoromethyl group; multicomponent reactions
资金
- National Natural Science Foundation of China [21072057]
- National Basic Research Program of China (973 Program) [2010CB126101]
- Shanghai Foundation of Science of Technology [09391911800]
- Shanghai Leading Academic Discipline Project [B507]
Fourteen difluoromethyl-containing 1,4-disubstituted 1,2,3-triazoles were synthesized via a novel copper-catalyzed click-multicomponent reaction of 2,2-difluoro-2-phenylsulfanylethanol, sodium azide and terminal alkynes in the presence of N-(p-toluenesulfonyl) imidazole, tetrabutylammonium iodide and triethylamine, followed by reductive cleavage of the phenylsulfanyl group using tributyltin hydride and azobisisobutyronitrile.
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