期刊
ADVANCED SYNTHESIS & CATALYSIS
卷 352, 期 14-15, 页码 2657-2662出版社
WILEY-V C H VERLAG GMBH
DOI: 10.1002/adsc.201000008
关键词
carbohydrates; glycosaminoglycans; glycosylation; hyaluronic acid; oligosaccharides
资金
- Deutsche Forschungsgemeinschaft [SPP1190]
Fully protected tetra-, hexa- and octasaccharides of hyaluronic acid were synthesized on a scale of several 100 mg up to gram quantities using allyl (methyl 2-O-benzoyl-3-O-benzyl-4-O-levulinoyl-beta-D-glucopyranosyluronate)-(1 -> 3)-4-O-acetyl-6-O-benzyl-2-deoxy-2-trichloroacetamido-beta-D-glucopyranoside as a key building block. This disaccharide was subjected to deprotection, then glycosylation via the trichloroacetimidate method was employed to achieve the formation of the oligosaccharides.
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