期刊
ADVANCED SYNTHESIS & CATALYSIS
卷 351, 期 11-12, 页码 1933-1938出版社
WILEY-V C H VERLAG GMBH
DOI: 10.1002/adsc.200900102
关键词
acetalization; carbon tetrabromide; organocatalysts; sodium triphenylphosphine-m-sulfonate; tetrahydropyranylation
资金
- Natural Science and Engineering Research Council (NSERC) of Canada
A solid complex, conveniently prepared from carbon tetrabromide and sodium triphenylphosphine-m-sulfonate (TPPMS), can be used as an easily recoverable catalyst for the selective acetalization of aldehydes and tetrahydropyranylation of alcohols. The catalyst can be recovered by simple precipitation with ether and can be reused at least 7 times without loss of catalytic activity.
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