期刊
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE
卷 65, 期 -, 页码 M780-U859出版社
INT UNION CRYSTALLOGRAPHY
DOI: 10.1107/S1600536809022077
关键词
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资金
- National Natural Science Foundation of China [20572018, 20672032]
- Heilongjiang Province [11531284, 1055HZ001, ZJG0504, JC200605]
- Heilongjiang University [09k137, 09k117, 09k118]
In the title heteronuclear complex, [CuTb(C19H2ON2O4)-(NO3)(3)(CH3COCH3)], the Cu-II ion is five-coordinated by two O and two N atoms from the 6,6'-dimethoxy-2,2'[propane-1,2-diylbis(nitrilomethylidyne)]diphenolate ligand (L) and an O atom from the acetone molecule in a square-pyramidal geometry. The Tb-III ion is ten-coordinated by six O atoms from three chelating nitrate ligands and four O atoms from the L ligand. In L, the CH2-CH-CH3 fragment is disordered over two conformations, with refined occupancies of 0.725 (11) and 0.275 (11).
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