期刊
ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS
卷 66, 期 -, 页码 m273-m275出版社
WILEY-BLACKWELL
DOI: 10.1107/S0108270110033135
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资金
- Ministry of Education, Youth and Sports of the Czech Republic [MSM 6046137301, 2B08021]
- Ministry of Industry and Trade of the Czech Republic [MPO 2A-2TP1/049]
The title compound, cis-diacetonitrile[(1R,2R)-1,2-diaminocyclohexane-kappa 2 N,N']platinum(II) dinitrate monohydrate, [Pt(C(2)H(3)N)(2)(C(6)H(14)N(2))](NO(3))(2)center dot H(2)O, is a molecular salt of the diaminocyclohexane-Pt complex cation. There are two formula units in the asymmetric unit. Apart from the two charge-balancing nitrate anions, one neutral molecule of water is present. The components interact via N-H...O and O-H...O hydrogen bonds, resulting in supramolecular chains. The title compound crystallizes only from acetonitrile with residual water, with the acetonitrile coordinating to the molecule of cis-[Pt(NO(3))(2)(DACH)] (DACH is 1,2-diaminocyclohexane) and the water forming a monohydrate.
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