期刊
ACS APPLIED MATERIALS & INTERFACES
卷 6, 期 5, 页码 3594-3599出版社
AMER CHEMICAL SOC
DOI: 10.1021/am405803z
关键词
thermoset epoxy; electrochromism; triphenylamine; near-infrared; triglycidyl isocyanurate; multicolored
资金
- National Science Council of Taiwan
In this study, two novel colorless thermoset epoxy resins with anodically electrochromism were prepared from the thermal curing of two triphenylamine-based diamine monomers, 4,4'-diamino-4-methoxytriphenylamine (1) and N,N'-bis(4-aminophenyl)-N,N'-di(4-methoxylphenyl)-1,4-phenylenediamine (2) with aliphatic epoxy triglycidyl isocyanurate, respectively. The resulting thermoset epoxy resins showed excellent softening temperature (T-s, 270 and 280 degrees C) due to the rigid structure and highly crosslinking density. In addition, novel colorless epoxy resin films revealed good reversible electrochemical oxidation and interesting multi-electrochromic behavior with high contrast ratio both in visible and near-infrared regions. The aliphatic thermoset epoxy resins also exhibited high transparency in visible region as colorless and great potential for practical electrochromic applications.
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