期刊
IUCRJ
卷 5, 期 -, 页码 190-199出版社
INT UNION CRYSTALLOGRAPHY
DOI: 10.1107/S2052252518000945
关键词
EIGER; hybrid pixel detectors; electron crystallography; SAPO-34
资金
- Swiss Nanoscience Institute [A11.04 HPD4FED]
Electron crystallography is a discipline that currently attracts much attention as method for inorganic, organic and macromolecular structure solution. EIGER, a direct-detection hybrid pixel detector developed at the Paul Scherrer Institut, Switzerland, has been tested for electron diffraction in a transmission electron microscope. EIGER features a pixel pitch of 75 x 75 mm(2), frame rates up to 23 kHz and a dead time between frames as low as 3 mu s. Cluster size and modulation transfer functions of the detector at 100, 200 and 300 keV electron energies are reported and the data quality is demonstrated by structure determination of a SAPO-34 zeotype from electron diffraction data.
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