期刊
ASIAN JOURNAL OF ORGANIC CHEMISTRY
卷 7, 期 7, 页码 1311-1314出版社
WILEY-V C H VERLAG GMBH
DOI: 10.1002/ajoc.201800202
关键词
benzamides; C-H activation; electrochemical oxidation; iodine; palladium
资金
- JSPS KAKENHI [15H05839, 16H01040, 17K19126]
- CREST from the Japan Science and Technology Agency (JST), Japan
- ACT-C from the Japan Science and Technology Agency (JST), Japan
- Grants-in-Aid for Scientific Research [15H05839, 17K19126, 16H01040] Funding Source: KAKEN
Palladium-catalyzed ortho-selective C-H iodination of N-(8-quinolinyl)benzamides proceeded using I-2 under both electrochemical and non-electrochemical conditions. The C-H iodination at 90 degrees C under base-free conditions provided high yields of the iodination products. The use of anodic oxidation increased the efficiency of the iodination at sterically-hindered positions.
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