期刊
VACUUM
卷 154, 期 -, 页码 159-166出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.vacuum.2018.05.008
关键词
a-C:H(Al); Bias voltage; Microstructure; Residual stress; Tribology
资金
- Project of the Scientific and Technical Foundation of Guangdong province [2014B050503005, 2017A070702016]
- Science and Technology Foundation of Guangdong Province [2017GDASCX-0202]
Al-doped hydrogenated amorphous carbon films were deposited by a hybrid deposition technique combining middle-frequency magnetron sputtering and anode layer ion source. The evolution of chemical composition, surface morphology and chemical bonding state of the resultant films were investigated using XPS, SEM, TEM and Raman spectroscopy, respectively. It was found that the surface morphology of as-deposited films evolved from a rough surface with quasi-columnar characteristic to an ultra-smooth surface with the increasing of applied bias voltage from 0 V to -400 V. At the low bias voltage of 0 V to -50 V, a polymer-like structure was mainly formed. A diamond-like structure is dominated at the moderate bias voltage of -100 V to -300 V, while it transforms to graphite-like after a further increase of the applied bias voltage up to -400 V. The residual stresses and tribological behavior were characterized by stress-tester and ball-on-disk tribo-meter, respectively. The results suggested that tensile stress or compressive stress of the a-C:H(Al) film can be tailored by modifying the applied bias voltage. Particularly, the film deposited at -150 V exhibited a combination of superior properties, including low residual stress, high hardness, a low steady-state friction coefficient of 0.045 and wear rate of 2.7 x 10(-7) mm(3) N-1.m(-1).
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