期刊
PHYTOCHEMISTRY LETTERS
卷 24, 期 -, 页码 75-78出版社
ELSEVIER
DOI: 10.1016/j.phytol.2018.01.002
关键词
Daphniphyllum paxianum; Daphniphyllum alkaloid; Structural elucidation
资金
- Lanzhou City University [LZCU-BS2015-06]
- Lanzhou City University key discipline foundation
- Lanzhou City University Young Teachers Research Projects Project of China [LZCU-QN2016-01, LZCU-QN2016-10]
A new daphniphyllum alkaloid daphnicyclidin M (1), containing one rare cyclopentadienyl anion, was isolated from the stems and leaves of Daphniphyllum paxianum Rosanth along with five known alkaloids, long-istylumphylline A (2), caldaphnidine A (3), caldaphnidine E (4), daphnilongeranin A (5), and 2-hydroxyyunnandaphnine D (6). The structures were elucidated on the basis of spectroscopic data, and the absolute configuration of 1 was assigned by single-crystal X-ray diffraction crystallography. The isolated compounds were found to have no antibacterial activity against Bacillus subtilis, Escherichia coll., Bacillus cereus, Staphylococcus aureus and Erwinia carotovora.
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