期刊
ORGANIC PROCESS RESEARCH & DEVELOPMENT
卷 22, 期 7, 页码 903-905出版社
AMER CHEMICAL SOC
DOI: 10.1021/acs.oprd.8b00151
关键词
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资金
- Independent Research Foundation Technology and Production [4148-00031]
- Danish National Research Foundation [DNRF118]
- Carlsberg Foundation [CF17-0517]
- Aarhus University
A simple setup has been devised to facilitate safer transfer of air-sensitive and pyrophoric reagents from Sure/Seal bottles in a fume hood setting. The setup is composed of three parts; a sealed transfer vial, a custom bottle cap for transfer vial alignment, and a metal clip. All of the needed parts are constructed from standard laboratory equipment and by 3D printing. Titration of tert-butyllithium was used as an example of safe transfer of a highly pyrophoric reagent, and an instructional video has been prepared.
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