期刊
ORGANIC LETTERS
卷 20, 期 13, 页码 4144-4147出版社
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.8b01776
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资金
- Robert A. Welch Foundation [F-0038]
- NIH-NIGMS [RO1-GM069445]
- UT Austin Center for Green Chemistry and Catalysis
- National Science Foundation [CHE 1361998, 1764380]
- Fundacao de Amparo a Pesquisa do Estado de Sao Paulo (FAPESP) [2017/00734-5, 2017/18487-4]
- China Scholarship Council [CSC.201707060020]
- Direct For Mathematical & Physical Scien
- Division Of Chemistry [1764380] Funding Source: National Science Foundation
Cyclometalated pi-allyliridium C,O-benzoates modified by (S)-SEGPHOS or (S)-Cl,OMe-BIPHEP catalyze enantioselective 2-propanol-mediated reductive couplings of diverse nonmetallic allyl pronucleophiles with the acetylenic aldehyde TIPSC CCHO. Absolute stereochemistries of the resulting secondary homoallylic-propargylic alcohols were assigned using Rychnovsky's competing enantioselective conversion method.
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