4.8 Article

Palladium-Catalyzed Decarbonylative Alkynylation of Amides

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ORGANIC LETTERS
卷 20, 期 9, 页码 2741-2744

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AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.8b00949

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  1. National NSF of China [21373080, 21403062, 21273067]
  2. NSF of Hunan Province [2016E1007]

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A palladium-catalyzed decarbonylative alkynylation of amides via C-N bond activation is developed. Compared with the reported Ni/Cu catalyzed reaction, which only proceeded well with silylacetylenes, this transformation was also applicable to both aromatic and aliphatic terminal alkynes, including those bearing functional groups, and thus provided a general and straightforward alkynes.

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