期刊
ORGANIC LETTERS
卷 20, 期 8, 页码 2172-2175出版社
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.8b00449
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资金
- Shaoxing University [21302130]
The first visible-light-mediated photoredox oxidative approach for generating carbamoyl radicals from oxamic acids is disclosed. Reaction of the generated carbamoyl radicals with electron-deficient alkenes opens efficient access to 3,4-dihydroquinolin-2(1H)-ones under mild conditions through a sequence of intermolecular radical addition,cyclization, and aromatization. The process is compatible with a variety of oxamic acids and electron-deficient alkenes, and a wide variety of 3,4-dihydroquinolin-2(1H)-ones were prepared.
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