期刊
MOLECULAR CRYSTALS AND LIQUID CRYSTALS
卷 664, 期 1, 页码 156-164出版社
TAYLOR & FRANCIS LTD
DOI: 10.1080/15421406.2018.1461837
关键词
Carbonyl substitution; crystal structure; diiron propanedithiolate; monophosphine ligand; synthesis
Two monosubstituted diiron complexes, namely (mu-SCH2CH2CH2S-mu)Fe-2(CO)(5)L (L = P(2-C4H3O)(3), 2; Ph2PCH2CH2CH3, 3), have been prepared by the carbonyl substitution of the parent complex (mu-SCH2CH2CH2S-mu)Fe-2(CO)(6) (1) with the corresponding monophosphine ligands in the presence of Me(3)NO2H(2)O. The new complexes were characterized by elemental analysis, spectroscopy and single crystal X-ray diffraction analysis.
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