期刊
MATERIALS RESEARCH BULLETIN
卷 98, 期 -, 页码 133-138出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.materresbull.2017.08.006
关键词
CoFe2O4; Sol-gel auto-combustion method; Ferrites; Magnetic properties
资金
- National Science Foundation of China (NSFC) [11604234, 51602214]
- Natural Science Foundation of Shanxi [201601D202010]
Cobalt ferrite powders were successfully synthesized by sol-gel auto-combustion method. Influence of sintering temperature on structural, magnetic and dielectric properties was studied. All the obtained samples are spinet ferrite with a cubic symmetry. As the sintering temperature increased from 900 degrees C to 1300 degrees C, the average grain size increased from 0.26 mu m to 0.83 mu m The dielectric constant and loss tangent measurement showed strong temperature dependence at all frequencies. The maximum magnetization increased while the coercivity and remanent magnetization decreased with the increasing sintering temperature. The non-saturation at high fields may be related to the surface effects in CoFe2O4 samples. When sintered at 1300 degrees C, the sample showed a maximum magnetization value of similar to 87.32 emu/g at room temperature. The highest value of coercivity of all the samples was 1368.33 Oe for the sample sintered at 900 degrees C. (C) 2017 Elsevier Ltd. All rights reserved.
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