期刊
JOURNAL OF THE EUROPEAN CERAMIC SOCIETY
卷 38, 期 14, 页码 4585-4589出版社
ELSEVIER SCI LTD
DOI: 10.1016/j.jeurceramsoc.2018.06.034
关键词
Ti(2)AIC; Ti3AlC2; MAX phase; Molten salt; Synthesis
资金
- EPSRC
- NNL Internal R&D Programme Centre for Advanced Fuels under the Industrial CASE scheme [1614290]
- Department of Energy and Climate Change
- EPSRC [EP/L018616/1, EP/M026566/1] Funding Source: UKRI
The molten salt method was used to synthesise the MAX phase compounds Ti2AlC and Ti3AlC2 from elemental powders. Between 900-1000 degrees C, Ti2AlC was formed alongside ancillary phases TiC and TiAl, which decreased in abundance with increasing synthesis temperature. Changing the stoichiometry and increasing the synthesis temperature to 1300 degrees C resulted in formation of Ti3AlC2 alongside Ti2AlC and TiC. The type of salt flux used had little effect on the product formation. The reaction pathway for Ti2AlC was determined to be the initial formation of TiCi. templating on the graphite and titanium aluminides.
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