期刊
JOURNAL OF THE EUROPEAN CERAMIC SOCIETY
卷 38, 期 2, 页码 687-693出版社
ELSEVIER SCI LTD
DOI: 10.1016/j.jeurceramsoc.2017.09.017
关键词
Transparent YAG ceramic; MgO additive; Grain growth; Densification; Optical property
资金
- Priority Academic Program Development of Jiangsu Higher Education Institutions (PAPD)
- National Natural Science Foundation of China [51402133, 61775088]
- Research and Innovation Program for College Graduates of Jiangsu Province [KYZZ16_0231]
- Special Project for Technology Innovation of Xuzhou City [KC16GZ014, KC16HQ236, KC16HQ237]
In current study, various amounts of MgO single dopant was adopted to fabricated high quality transparent YAG ceramics, by utilizing a simple one-step solid state reaction sintering method in vacuum. At a MgO doping amount of only 0.03 wt.%, YAG transparent ceramics with a transmittance of 84.5% at 1064 nm could be obtained, after sintering at 1820 degrees C for 8 h. The microstructure evolution and optical property of as-fabricated YAG ceramics as a function of MgO doping concentration were systematically investigated. MgO dopant could effectively promote densification of YAG ceramics when the sintering temperature was lower than 1660 degrees C, and dramatically accelerate its grain growth between 1540 degrees C and 1660 degrees C. Further increase the doping amount of MgO would not benefit to the optical quality of YAG ceramics, and the intragranular pores as well as the Mg-riched secondary phase were observed from the MgO heavily doped ceramics.
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