期刊
CHEMICAL PAPERS
卷 68, 期 3, 页码 384-391出版社
DE GRUYTER OPEN LTD
DOI: 10.2478/s11696-013-0449-y
关键词
cannabisin F; lignanamide; 8-O-4 '-neolignan; tyramine
资金
- National Natural Science Foundation of Shandong [ZR2010 HM023]
- Chinese Medicine Administration Bureau of the Gansu Province [GZK-2011-62]
A practical eight-step synthesis of lignanamide cannabisin F starting from vanillin is reported for the first time. This synthetic strategy applies the aldol reaction followed by the Wittig reaction to afford the key 8-O-4'-neolignan intermediate diacid. The diacid was condensed with N,O-protected tyramine giving, after deprotection, cannabisin F.
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