期刊
JOURNAL OF RADIOANALYTICAL AND NUCLEAR CHEMISTRY
卷 317, 期 1, 页码 565-570出版社
SPRINGER
DOI: 10.1007/s10967-018-5919-9
关键词
Environmental radioactivity; Plants; Pb-210; Microwave digestion; Liquid scintillation counting
资金
- National Natural Science Foundation of China [11575178]
Pb-210, a highly-toxic radionuclide, is widely distributed in environments and is commonly the target for monitoring. In this paper, a modified method for determining Pb-210 radioactivities in plants in China has been presented. The procedure involves digesting the plant samples by microwave directly, separating Pb-210 from Bi-210 and Po-210 with Sr resins, and measuring the beta particles using liquid scintillation counting (LSC). Compared to previously reported approaches, this method uses no hydrochloric acids which are restricted in China and involves no co-precipitation. The entire procedure could be finished within 1 day with a radiochemical yield of 70%. The lower limit of detection for Pb-210 was found to be 38.0 mBq/g for a counting time of 72,000 s. The method was tested using a standard solution and plant samples. LSC spectra indicate that Pb-210 is effectively stripped and the results are consistent with those obtained from the gamma-spectrometry.
作者
我是这篇论文的作者
点击您的名字以认领此论文并将其添加到您的个人资料中。
推荐
暂无数据