期刊
JOURNAL OF ORGANIC CHEMISTRY
卷 83, 期 12, 页码 6754-6761出版社
AMER CHEMICAL SOC
DOI: 10.1021/acs.joc.8b00674
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资金
- NSFC [21772163, 21778042, 21375113]
- NFFTBS [J1310024]
- Fundamental Research Funds for the Central Universities [20720160030]
The first oxidative C(sp(3))-H phosphonylation of tertiary aliphatic amines has been developed. The use of cobalt acetate as a catalyst, N-hydroxyphthalimide as a cocatalyst, and air as an oxidant enabled the conversion of tertiary aromatic and aliphatic amines into alpha-aminophosphonates in moderate to excellent yields under mild conditions via a cross dehydrogenative coupling reaction.
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