In-Process Monitoring of Material Cross-Contamination Defects in Laser Powder Bed Fusion

The goal of this work is to detect the onset of material cross-contamination in laser powder bed fusion (L-PBF) additive manufacturing (AM) process using data from in situ sensors. Material cross-contamination refers to trace foreign materials that may be introduced in the powder feedstock used in the process due to reasons such as poor cleaning of the machine after previous builds or inadequate quality control during production and storage of the powder. Material cross-contamination may lead to deleterious changes in the microstructure of the AM part and consequently affect its functional properties. Accordingly, the objective of this work is to develop and apply a spectral graph theoretic approach to detect the occurrence of material cross-contamination in real-time as the part is being built using in-process sensors. The central hypothesis is that transforming the process signals in the spectral graph domain leads to early and more accurate detection of material cross-contamination in L-PBF compared to the traditional delay-embedded Bon-Jenkins stochastic time series analysis techniques, such as autoregressive (AR) and autoregressive moving average (ARMA) modeling. To test this hypothesis, Inconel alloy 625 (UNS alloy 06625) test parts were made at Edison Welding Institute (EWI) on a custom-built L-PBF apparatus integrated with multiple sensors, including a silicon photodetector (with 300 nm to 1100 nm optical wavelength). During the process, two types of foreign contaminant materials, namely, tungsten and aluminum particulates, under varying degrees of severity were introduced. To detect cross-contamination in the part, the photodetector sensor signatures were monitored hatch-by-hatch in the form of spectral graph transform coefficients. These spectral graph coefficients are subsequently tracked on a Hotelling T-2 statistical control chart. Instances of Type II statistical error, i.e., probability of failing to detect the onset of material cross-contamination, were verified against X-ray computed tomography (XCT) scans of the part to be within 5% in the case of aluminum contaminant particles. In contrast, traditional stochastic time series modeling approaches, e.g., ARMA, had corresponding Type II error exceeding 15%. Furthermore, the computation time for the spectral graph approach was found to be less than one millisecond, compared to nearly 100 ms for the traditional time series models tested.