期刊
JOURNAL OF CHROMATOGRAPHIC SCIENCE
卷 56, 期 4, 页码 336-343出版社
OXFORD UNIV PRESS INC
DOI: 10.1093/chromsci/bmy003
关键词
-
资金
- Manisa Celal Bayar University Research Foundation Project [2015-064]
A simple method was validated for the analysis of 31 phenolic compounds using liquid chromatography-electrospray tandem mass spectrometry. Proposed method was successfully applied to the determination of phenolic compounds in an olive leaf extract and 24 compounds were analyzed quantitatively. Olive biophenols were extracted from olive leaves by using microwave-assisted extraction with acceptable recovery values between 78.1 and 108.7%. Good linearities were obtained with correlation coefficients over 0.9916 from calibration curves of the phenolic compounds. The limits of quantifications were from 0.14 to 3.2 mu g g(-1). Intra-day and inter-day precision studies indicated that the proposed method was repeatable. As a result, it was confirmed that the proposed method was highly reliable for determination of the phenolic species in olive leaf extracts.
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