期刊
JOURNAL OF CEREAL SCIENCE
卷 82, 期 -, 页码 65-72出版社
ACADEMIC PRESS LTD- ELSEVIER SCIENCE LTD
DOI: 10.1016/j.jcs.2018.04.005
关键词
Portable mid-infrared spectroscopy; Andean flour; Authentication; Quinoa; Kaniwa; Amaranth
Quinoa (Chenopodium quinoa Willd.), kaniwa (Chenopodium pallidicaule Aellen) and kiwicha (amaranth, Chenopodium pallidicaule) are high nutritional value grains that are at risk for adulteration with less expensive grains. Our objective was to develop a rapid untargeted approach to authenticate high-value Andean grain flours by combining infrared spectroscopy and pattern recognition analysis. Samples (n = 106) were collected from Peruvian (n = 89) and US (n = 17) markets that included quinoa, amaranth, kahiwa and other common flours from the Andean region. Flour composition was characterized by reference methods including fat (Soxhlet, AOAC#922.06), protein (Dumas, ICC Standard #167), and fatty acid profile (AOAC #996.0). Spectra was collected by using a portable infrared system with a single-reflection diamond ATR crystal, and analyzed by Soft Independent Model of Class Analogies and Partial Least Square Regression. Authentic grain flours formed distinct clusters and commercial samples from Peruvian markets showed a prevalence of adulteration. Spectral differences were associated with the fingerprint region (1100-900 cm(-1)) due to differences in starch structure. Regression models were generated for rapid determination of fat (Rcv = 0.98, SECV = 0.3) and protein (Rcv = 0.98, SECV = 0.96) levels. New generation of portable infrared devices provided a viable tool for chemical profiling allowing for rapid, in-field, and reliable authentication of food ingredients. (C) 2018 Elsevier Ltd. All rights reserved.
作者
我是这篇论文的作者
点击您的名字以认领此论文并将其添加到您的个人资料中。
推荐
暂无数据