期刊
JOURNAL OF ALLOYS AND COMPOUNDS
卷 762, 期 -, 页码 282-288出版社
ELSEVIER SCIENCE SA
DOI: 10.1016/j.jallcom.2018.05.171
关键词
Ceramics; Dielectric response; X-ray diffraction; Electron paramagnetic resonance; Solid state reactions
资金
- National Natural Science Foundations of China [21271084]
- Jilin Province [20160101290JC]
- Changbai Mountain Scholar Distinguished Professor [2015047]
(Ba1-xDyx) (Ti1-x/2Cax/2)O-3 (BDTC) ceramics were prepared at 1400 degrees C using the solid-state reaction method. The solubility limit was determined by XRD to be x =0.15. The BDTC ceramic with x =0.10 exhibited a high relative density (95%), a fine-grained microstructure (1.2 mu m), X8R dielectric stability (vertical bar(epsilon' - epsilon'(RT)vertical bar/epsilon'(RT) <= 15% in a range -55 to 150 degrees C), and a lower loss (tan delta < 0.02) below 2 x 10(4) Hz. Ferroelectric and paraelectric phases coexist in a wide temperature region. The mixed A and B occupancy for Dy3+ and Ca2+ ions was proposed to be responsible for the X8R stability associated with double diffused dielectric peaks. (C) 2018 Elsevier B.V. All rights reserved.
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