期刊
FOOD CHEMISTRY
卷 260, 期 -, 页码 174-182出版社
ELSEVIER SCI LTD
DOI: 10.1016/j.foodchem.2018.04.007
关键词
Endocrine disrupting compounds; QuEChERS; Air-assisted liquid-liquid microextraction; Fish; High-performance liquid; chromatography-tandem mass spectrometry
资金
- National Special Fund for Agroscientific Research in the Public Interest [201503108]
- Science & Technology Project of Hunan Province [2017WK2091]
A new, sensitive, and rapid method based on the Quick, Easy, Cheap, Effective, Rugged and Safe (QuEChERS) approach and air-assisted liquid-liquid microextraction (AALLME) technology was developed for the determination of 20 endocrine-disrupting compounds (EDCs) in fish by high-performance liquid chromatography-tandem mass spectrometry. The method first integrates AALLME into QuEChERS to achieve clean-up and enrichment of the EDCs in one step. A self-made glass tube was enfolded with plasticine to withstand the high centrifugal force. The established method was developed by optimization of the parameters. High linearities (R-2 > 0.9924) and recoveries (78.2-118.6%) at three spiked levels (5, 10, and 20 ng g(-1)), and low relative standard deviation values (1.1-14.5%) and limits of detection (0.03-0.80 ng g(-1)) were obtained. The method comparison shows that the proposed method is superior as it involves less organic solvent usage, simple operation and high efficiency. This method was successfully applied to different fishes for analyzing EDCs.
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